不對稱有機催化反應金雞納生物堿衍生物催化不對稱“中斷的”feistb233;nary反應_第1頁
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1、第四軍醫(yī)大學博士學位論文 0目 錄 縮略語表································

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3、#183;····································

4、;····1 中文摘要·······························

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6、#183;····································

7、;·····3 英文摘要······························

8、83;····································&

9、#183;····································

10、;······7 第一章 文獻綜述 ····························

11、3;····································&#

12、183;····························11 第二章 正文 ······&#

13、183;····································

14、····································

15、3;······················37 2.1 金雞納生物堿酯類衍生物的合成及其在不對稱 IFB 反應中的應用····37 2.2 金雞納生物堿醚類衍生物的合成及其在

16、不對稱 IFB 反應中的應用····49 2.3 金雞納生物堿胺類衍生物的合成及其在不對稱 IFB 反應中的應用····56 2.4 金雞納生物堿硫脲類衍生物的合成及其在不對稱 IFB 反應中的應用 64 2.5 金雞納生物堿衍生物催化不對稱 IFB 反應的機理 ········

17、·······················71 第三章 實驗部分 ···········

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19、183;····································

20、·········73 全文總結··························

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22、#183;····································

23、;······101 參考文獻·····························&

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26、83;···103 附 錄 ·······························&#

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28、····································

29、3;···························120 個人簡歷和研究成果 ·······

30、····································

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32、183;·····136 致謝······························

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34、3;····································&#

35、183;··········138 第四軍醫(yī)大學博士學位論文 2PMP p-methoxypheyl 對甲氧基苯基 pKa 電離平衡常數(shù)負對數(shù) PPA polyphosphoric acid 多聚磷酸 PS Proton Sponge 質子海綿 SN2 nucleophilic substitution reaction

36、雙分子親核加成反應 QN quinine 奎寧 QD quinidine 奎尼定 THF tetrahydrofuran 四氫呋喃 TLC thin layer chromatography 薄層色譜法 Ts 4-toluene sulfonyl 對甲苯磺?；?TsOH 4-toluenesulfonic acid 對甲基苯磺酸 % ee percent enantiomeric excess 百分對映體過量

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